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By Anil K. Mukherji, R. Belcher and M. Frieser (Auth.)

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And RAGHAVA RAO, B. S. , / . Indian Chem. Soc. 28, 257 (1951). 102. RYAN, D . , Canadian J. Chem. 38, 2488 (1960). 103. ALIMARIN, I. P. and TUNG-SCHAING, TSE, Talanta, 9, 9 (1962). 104. 105. 106. 107. 108. 109. 110. 111. 112. BAIULESCU, G. , Anal. Chim. Acta, 21, 33 (1959). ELVING, P. J. and OLSON, E. C , Anal Chem. 27, 1817 (1955). LUNDELL, G. E. F. and KNOWLES, H. , Ind. Engng. Chem. 12, 344 (1920). , Z. Anorg. Chem. 72, 89 (1911). SMITH, G. , Cupferron and Neocupferron, G. F. Smith, Columbus, Ohio, 1938.

Following procedures are recommended : Procedure Add sufficient hydrochloric acid (5-6 M final acid concentration) to a 100 ml solution containing 5-150 mg Zr. Add 10-12 g of hydroxylpropylmandelate syrup mixture (88 % in methanol) with stirring. Digest at 80°C on a hot plate for about 3 hr. The determination can be concluded by either of the following methods : (a) Filter the hot mixture through a medium porosity ignition crucible, washing the precipitate with no more than 150 ml of hot wash solution (5 % mandelic acid solution in 2 % HC1).

24, 1861 (1952). ALIMARIN, I. P. and HAN-SI, SHEN, Zhur. Anal. Khim. 16, 279 (1961). HAHN, R. B. and JOSEPH, P. , Anal. Chem. 28, 2019 (1956). 101. VENKATARAMANIAH, M. and RAGHAVA RAO, B. S. , / . Indian Chem. Soc. 28, 257 (1951). 102. RYAN, D . , Canadian J. Chem. 38, 2488 (1960). 103. ALIMARIN, I. P. and TUNG-SCHAING, TSE, Talanta, 9, 9 (1962). 104. 105. 106. 107. 108. 109. 110. 111. 112. BAIULESCU, G. , Anal. Chim. Acta, 21, 33 (1959). ELVING, P. J. and OLSON, E. C , Anal Chem. 27, 1817 (1955).

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