By Robert E. Sievers
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703(6) Non-equivalent coordination polyhedra of Eu(thd) 3(DMF) 2. 6(2) 03. 3(2) . 730(6) Figure 1 0 . 04 03. 2742(6) Non-equivalent coordination polyhedra of Eu(thd) 3(DMSO). 51 M A G N E T I C A N I S O T R O P Y AND D I P O L A R S H I F T S SHIFT William REAGENT DeW. H o r r o c k s IN SYSTEMS J r . , James P. Sipe, I I I and Oanïeï~3u3nïcK Department of Chemistry, University, I· University The P e n n s y l v a n i a Park, Penna. State 16802 Introduction II. Survey I I I . Solid IV. Direct of Action State Evaluation Anisotropy V.
S e v e r a l t r e n d s a p p e a r i n t h e d a t a w h i c h may b e e x p l a i n e d on t h e b a s i s of r e l a t i v e n u c l e o p h i l i c i t i e s a n d s t e r i c c o n s t r a i n t s of t h e i n t e r a c t i o n s . These t r e n d s have b e e n s u m m a r i z e d i n t e r m s of f o u r e f f e c t s : chain l e n g t h e n i n g , f u n c t i o n a l group p o s i t i o n , b r a n c h i n g , and c y c l i z a tion. Chain L e n g t h The d a t a i n d i c a t e t h a t , a s a g e n e r a l r u l e , i n c r e a s i n g t h e l e n g t h of t h e a l k y l c h a i n i n a s e r i e s of s i m i l a r comp o u n d s i n c r e a s e s t h e s t a b i l i t y of t h e complex f o r m e d .
These t r e n d s have b e e n s u m m a r i z e d i n t e r m s of f o u r e f f e c t s : chain l e n g t h e n i n g , f u n c t i o n a l group p o s i t i o n , b r a n c h i n g , and c y c l i z a tion. Chain L e n g t h The d a t a i n d i c a t e t h a t , a s a g e n e r a l r u l e , i n c r e a s i n g t h e l e n g t h of t h e a l k y l c h a i n i n a s e r i e s of s i m i l a r comp o u n d s i n c r e a s e s t h e s t a b i l i t y of t h e complex f o r m e d . f For example, t h e K v a l u e s f o r 2 - p r o p a n o l , 2 - b u t a n o l , 2 p e n t a n o l , 2 - h e x a n o l , and 2 - h e p t a n o l a r e 2 0 .