By G. Svehla
Spot exams are outlined as an analytical method which permits the analyst to complete passable semi-micro, micro and ultra-micro checks with basic gear and minimal intake of pattern and time. those easy checks utilize the colour and scent of the natural compound within the initial degree of study and likewise the id of convinced vapors and gases developed in the course of pyrolysis. quantity X comprises chapters. the 1st, on natural spot try research, is complementary to P.W. West’s shorter bankruptcy on inorganic spot try systems, released in quantity IA greater than two decades in the past. the second one bankruptcy provides a quick heritage of analytical chemistry. along with being a useful resource of references to early analytical paintings, this bankruptcy makes such a lot a laugh interpreting.
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Extra resources for Organic Spot Test Analysis The History of Analytical Chemistry
C h e m . , 3 1 ( 1 9 5 9 ) 2 0 9 9 . D . D a v i d s o n , J. C h e m . E d u c , 1 9 ( 1 9 4 2 ) 2 2 1 , 5 3 2 . F . F e i g l , C. C o s t a N e t o a n d G . E . R . M a r i n s , s e e F . F e i g l a n d V . A n g e r , S p o t Tests in Organic Analysis, Elsevier, A m s t e r d a m , 7 t h e d n . , 1 9 6 6 , p. 1 0 8 . F. Feigl, V. G e n t i l a n d G . E . R . Marins, s e e F. Feigl a n d V. A n g e r , S p o t T e s t s in Organic Analysis, Elsevier, A m s t e r d a m , 7 t h e d n . , 1 9 6 6 , p.
C o s t a N e t o , s e e F . F e i g l a n d V . , 1 9 6 6 , p. 3 3 7 . G. K u n o v i t z , A n a l . C h i m . A c t a , 5 5 ( 1 9 7 1 ) 2 2 1 . G. K u n o v i t z , A n a l . C h i m . A c t a , 7 0 ( 1 9 7 4 ) 2 1 3 . T . N a k a i , T. O h t a a n d M. T a k a y a m a , A g r i c . B i o l . C h e m . , 3 8 ( 1 9 7 4 ) 1 2 0 9 . 76 Y . A s a b e , K. N u m a t a , D . S u z u k i a n d S. T a k i t a n i , B u n s e k i K a g a k u , 2 4 ( 1 9 7 5 ) 60 61 62 63 64 65 66 67 68 69 70 71 72 81 82 160.
5 μg glycerol. (33) Malonic acid In a micro test tube (a) 1 drop of the test solution is treated with (b) several drops of a saturated methanolic solution of urea. After evaporation of the alcohol, the tube is heated for several minutes in a glycerol bath at 120° C. (c) 1 Drop of a 1% solution of pyridylpyridinium dichloride in dimethylformamide is added. The mixture is heated at 120°C for several minutes. In the presence of malonic acid, a reddish-blue color develops on cooling, which fluoresces red under UV light.